![](/CAS/GIF/111-68-2.gif)
1-AMINOHEPTANE synthesis
- Product Name:1-AMINOHEPTANE
- CAS Number:111-68-2
- Molecular formula:C7H17N
- Molecular Weight:115.22
![1-Bromoheptane](/CAS/GIF/629-04-9.gif)
629-04-9
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$7.00/10g
![1-AMINOHEPTANE](/CAS/GIF/111-68-2.gif)
111-68-2
122 suppliers
$14.00/1mL
Yield:111-68-2 85%
Reaction Conditions:
with 5-methyl-1,3,4-thiadiazol-2-amine;triethylamine in ethanol;water at 25; for 1 h;
Steps:
Typical experimental procedure for primary amines synthesis
General procedure: A mixture of alkyl halide (1.0 mmol) and 5-methyl-1,3,4-thiadiazole-2-amine (1) (1.5 mmol) were added to a flaskcontaining 3 mmol Et3N and 2 cm3 EtOH/H2O (10:1). The reaction continued at room temperature under atmosphericconditions 1 h. The reaction progress was controlled by thin-layer chromatography. Then, crude reaction mixture was purified by column chromatography (petroleum ether/ethyl acetate 1:4) to give the primary amines in good yields.
References:
Soleiman-Beigi, Mohammad;Mohammadi, Fariba [Monatshefte fur Chemie,2017,vol. 148,# 12,p. 2123 - 2128]
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629-08-3
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$70.00/1g
![1-AMINOHEPTANE](/CAS/GIF/111-68-2.gif)
111-68-2
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$14.00/1mL
![heptanal oxime](/CAS/GIF/629-31-2.gif)
629-31-2
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![1-AMINOHEPTANE](/CAS/GIF/111-68-2.gif)
111-68-2
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![1-NITROHEPTANE](/CAS/GIF/693-39-0.gif)
693-39-0
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![1-AMINOHEPTANE](/CAS/GIF/111-68-2.gif)
111-68-2
122 suppliers
$14.00/1mL