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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide

1-Benzyl-4-(4-methylphenyl)tetrahydropyridine synthesis

8synthesis methods
3612-20-2 Synthesis
N-Benzyl-4-piperidone

3612-20-2
486 suppliers
$6.00/10g

4-Chlorotoluene

106-43-4
330 suppliers
$14.00/5g

1-Benzyl-4-(4-methylphenyl)tetrahydropyridine

13314-67-5
20 suppliers
inquiry

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Yield:13314-67-5 93%

Reaction Conditions:

Stage #1: 1-phenylmethyl-4-piperidonewith tris-(dibenzylideneacetone)dipalladium(0);toluene-4-sulfonic acid hydrazide;lithium tert-butoxide;XPhos in 1,4-dioxane; for 0.0166667 h;Inert atmosphere;
Stage #2: para-chlorotoluene in 1,4-dioxane at 110; for 5 h;Inert atmosphere;

References:

Barluenga, Jose;Tomas-Gamasa, Maria;Moriel, Patricia;Aznar, Fernando;Valdes, Carlos [Chemistry - A European Journal,2008,vol. 14,# 16,p. 4792 - 4795] Location in patent:supporting information; scheme or table

50-00-0 Synthesis
Formaldehyde

50-00-0
846 suppliers
$10.00/25g

4-Tolylboronic acid

5720-05-8
425 suppliers
$5.00/1g

N-benzylbut-3-yn-1-amine

107301-61-1
2 suppliers
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1-Benzyl-4-(4-methylphenyl)tetrahydropyridine

13314-67-5
20 suppliers
inquiry

References
Methanesulfonic acid, 1,1,1-trifluoro-, 1,2,3,6-tetrahydro-1-(phenylmethyl)-4-pyridinyl ester

126781-38-2
0 suppliers
inquiry

4-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)TOLUENE

195062-57-8
148 suppliers
$5.00/250mg

1-Benzyl-4-(4-methylphenyl)tetrahydropyridine

13314-67-5
20 suppliers
inquiry

References
4-Piperidinol, 4-(4-methylphenyl)-1-(phenylmethyl)-

13299-35-9
3 suppliers
inquiry

1-Benzyl-4-(4-methylphenyl)tetrahydropyridine

13314-67-5
20 suppliers
inquiry

References
3612-20-2 Synthesis
N-Benzyl-4-piperidone

3612-20-2
486 suppliers
$6.00/10g

4-Bromotoluene

106-38-7
391 suppliers
$14.00/5g

1-Benzyl-4-(4-methylphenyl)tetrahydropyridine

13314-67-5
20 suppliers
inquiry

References

1-Benzyl-4-(4-methylphenyl)tetrahydropyridine Related Search:

Benzyl benzoate 2,4,6-Collidine Benzyl chloride Benzyl alcohol Benzyl nicotinate 2,6-Lutidine 2-Chloro-5-(chloromethyl)pyridine Benzyl isocyanate Dimethylbenzylcarbinyl acetate 1-BENZYL-1,2,3,6-TETRAHYDRO-4-PHENYLPYRIDINE