![](/CAS/20120318/GIF/CB52578300.gif)
1-Chloro-3-(1-chloro-ethyl)-benzene synthesis
- Product Name:1-Chloro-3-(1-chloro-ethyl)-benzene
- CAS Number:34887-78-0
- Molecular formula:C8H8Cl2
- Molecular Weight:175.06
![1-Chloro-3-ethylbenzene](/CAS/GIF/620-16-6.gif)
620-16-6
76 suppliers
$60.00/500mg
![1-CHLORO-3- (2-CHLORO-ETHYL)-BENZENE](/CAS/GIF/5182-43-4.gif)
5182-43-4
11 suppliers
inquiry
![1-Chloro-3-(1-chloro-ethyl)-benzene](/CAS/20120318/GIF/CB52578300.gif)
34887-78-0
8 suppliers
$45.00/10mg
Yield:34887-78-0 71% ,5182-43-4 23 %Spectr.
Reaction Conditions:
with N-chloro-succinimide;benzophenone in acetonitrile at 27; for 9 h;Irradiation;regioselective reaction;
Steps:
4 General procedure for triplet ketone-catalyzed C(sp3)-H-chlorination
General procedure: To a 4 mL clear vial charged with the reaction substrate, N-chlorosuccinimide, ketone catalyst in anhydrous acetonitrile (0.2 M) was degassed and irradiated with a 19 W compact fluorescent lamp at room temperature for 24 h. The solvent was then removed and the residue was dissolved in diethyl ether, filtrated, concentrated and purified by preparative thin-layer chromatography.
References:
Han, Lei;Xia, Ji-Bao;You, Lin;Chen, Chuo [Tetrahedron,2017,vol. 73,# 26,p. 3696 - 3701]
![3-Chlorostyrene](/CAS/GIF/2039-85-2.gif)
2039-85-2
167 suppliers
$11.00/1g
![1-Chloro-3-(1-chloro-ethyl)-benzene](/CAS/20120318/GIF/CB52578300.gif)
34887-78-0
8 suppliers
$45.00/10mg
![1-Chloro-3-ethylbenzene](/CAS/GIF/620-16-6.gif)
620-16-6
76 suppliers
$60.00/500mg
![1-Chloro-3-(1-chloro-ethyl)-benzene](/CAS/20120318/GIF/CB52578300.gif)
34887-78-0
8 suppliers
$45.00/10mg
![Chlorobenzene](/CAS/GIF/108-90-7.gif)
108-90-7
643 suppliers
$10.00/25G
![1-Chloro-3-(1-chloro-ethyl)-benzene](/CAS/20120318/GIF/CB52578300.gif)
34887-78-0
8 suppliers
$45.00/10mg
![3-BROMOCHLOROBENZENE](/CAS/GIF/108-37-2.gif)
108-37-2
352 suppliers
$6.00/10g
![1-Chloro-3-(1-chloro-ethyl)-benzene](/CAS/20120318/GIF/CB52578300.gif)
34887-78-0
8 suppliers
$45.00/10mg