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1-CHLORO-3- (2-CHLORO-ETHYL)-BENZENE synthesis

13synthesis methods
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Yield:5182-43-4 91%

Reaction Conditions:

Stage #1: 2-(3-chlorophenyl)ethanolwith methanesulfonyl chloride;triethylamine in toluene at 0; for 1 h;
Stage #2: with lithium chloride in N,N-dimethyl-formamide at 20; for 24 h;

References:

Yus, Miguel;Ramón, Diego J.;Gómez, Inmaculada [Journal of Organometallic Chemistry,2002,vol. 663,# 1-2,p. 21 - 31]

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