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ChemicalBook CAS DataBase List 1-ETHYL-4-METHYLQUINOLINIUM IODIDE
605-59-4

1-ETHYL-4-METHYLQUINOLINIUM IODIDE synthesis

3synthesis methods
-

Yield:605-59-4 96%

Reaction Conditions:

in acetonitrile; for 6 h;Reflux;

Steps:

2.1 Example 2

(1) Take 3g of 4-methylquinoline into a 100 ml flask, and 50 ml of dry acetonitrile was added. After the dissolution, 3.9 g of iodoethane was added, and the mixture was reacted under heating and reflux for 6 hours. After completion of the reaction, most of the acetonitrile was removed under reduced pressure distillation, product was poured into anhydrous ethyl ether and a yellow solid precipitated. After suction filtration, the filter cake was washed three times with anhydrous ethyl ether to give a pure product, yield 96%.

References:

CN108410202,2018,A Location in patent:Paragraph 0002

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