1-ETHYL-4-METHYLQUINOLINIUM IODIDE synthesis
- Product Name:1-ETHYL-4-METHYLQUINOLINIUM IODIDE
- CAS Number:605-59-4
- Molecular formula:C12H14IN
- Molecular Weight:299.15
Yield:605-59-4 96%
Reaction Conditions:
in acetonitrile; for 6 h;Reflux;
Steps:
2.1 Example 2
(1) Take 3g of 4-methylquinoline into a 100 ml flask, and 50 ml of dry acetonitrile was added. After the dissolution, 3.9 g of iodoethane was added, and the mixture was reacted under heating and reflux for 6 hours. After completion of the reaction, most of the acetonitrile was removed under reduced pressure distillation, product was poured into anhydrous ethyl ether and a yellow solid precipitated. After suction filtration, the filter cake was washed three times with anhydrous ethyl ether to give a pure product, yield 96%.
References:
CN108410202,2018,A Location in patent:Paragraph 0002
62-53-3
675 suppliers
$10.00/1g
605-59-4
38 suppliers
$378.00/5g
607-66-9
186 suppliers
$8.00/5g
605-59-4
38 suppliers
$378.00/5g