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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
ChemicalBook CAS DataBase List 1-Propanesulfonyl chloride

1-Propanesulfonyl chloride synthesis

9synthesis methods
2,4,6-Trichloro-[1,3,5]-triazine (TCT) was added at room temperature to a solution of propane-1-sulfonic acid in acetone dry, followed by NEt3 dropwise. The resulting mixture was irradiated to 80 °C (50 W of MW power) for 20 min in a sealed tube (10 mL pressure-rated reaction vial) in a self-tuning single-mode irradiating synthesizer. The mixture was cooled rapidly to room temperature by passing compressed air through the microwave cavity for 1 min. After cooling to room temperature, the precipitate was filtered off on Celite to afford 1-Propanesulfonyl chloride[1].
1-Propanesulfonyl chloride
Propyl disulfide

629-19-6
298 suppliers
$13.00/5g

1-Propanesulfonyl chloride

10147-36-1
202 suppliers
$5.00/5g

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Yield:10147-36-1 98%

Reaction Conditions:

with chloro-trimethyl-silane;potassium nitrate in dichloromethane at 50; for 4 h;

References:

Prakash, G. K. Surya;Mathew, Thomas;Panja, Chiradeep;Olah, George A. [Journal of Organic Chemistry,2007,vol. 72,# 15,p. 5847 - 5850]

5284-66-2 Synthesis
1-Propanesulfonic acid

5284-66-2
93 suppliers
$76.00/1g

1-Propanesulfonyl chloride

10147-36-1
202 suppliers
$5.00/5g

References
4253-91-2 Synthesis
N-PROPYL SULFOXIDE

4253-91-2
24 suppliers
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1-Propanesulfonyl chloride

10147-36-1
202 suppliers
$5.00/5g

References
Propyl thiocyanate

4251-16-5
24 suppliers
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1-Propanesulfonyl chloride

10147-36-1
202 suppliers
$5.00/5g

References
Sodium 1-propanesulfonate

14533-63-2
148 suppliers
$33.00/1g

1-Propanesulfonyl chloride

10147-36-1
202 suppliers
$5.00/5g

References

1-Propanesulfonyl chloride Related Search:

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