1-TERT-BUTOXY-2-PROPANOL synthesis
- Product Name:1-TERT-BUTOXY-2-PROPANOL
- CAS Number:57018-52-7
- Molecular formula:C7H16O2
- Molecular Weight:132.2
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Yield: 84.8%
Reaction Conditions:
with Amberlyst15 in hexane at 40; for 7 h;
Steps:
1
100.0 g (1.33 mol) of 1,2-propanediol, 84.9 g (0.66 mol) of a strongly acidic ion exchange resin, 200.0 g of hexane and tert-butyl alcohol 196 were added to a flask equipped with a stirrer. 9 g (2.66 mol), and the mixture was stirred at 40 ° C. for 7 hours. The resulting reaction solution was filtered and the filtrate was analyzed by GC. As a result, the composition of the reaction solution was 4.6% for 1,2-propanediol, 84.8% for 1-PTB, and 2.4% for DTBP There was DTBP / 1-PTB = 0.028.
References:
Koei ChemicalCo., Ltd.;Yamauchi, Hayato;Kawamichi, Takehide;Inoue, Naoto JP2016/108252, 2016, A Location in patent:Paragraph 0026
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