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ChemicalBook CAS DataBase List PHENYL 4-OXO-2-PHENYL-3,4-DIHYDROPYRIDINE-1(2H)-CARBOXYLATE
107971-39-1

PHENYL 4-OXO-2-PHENYL-3,4-DIHYDROPYRIDINE-1(2H)-CARBOXYLATE synthesis

5synthesis methods
-

Yield:107971-39-1 83%

Reaction Conditions:

Stage #1: 4-methoxypyridine;phenyl chloroformate in tetrahydrofuran at -23;
Stage #2: phenylmagnesium bromide in tetrahydrofuran;
Stage #3: Acidic conditions;

References:

McCall, W. Stephen;Grillo, Teresa Abad;Comins, Daniel L. [Organic Letters,2008,vol. 10,# 15,p. 3255 - 3257] Location in patent:scheme or table