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Benzeneacetic acid, 2-bromo-α-methylene-, methyl ester synthesis

4synthesis methods
18698-97-0 Synthesis
2-Bromophenylacetic acid

18698-97-0
333 suppliers
$10.00/1g

Benzeneacetic acid, 2-bromo-α-methylene-, methyl ester

1203555-34-3
2 suppliers
inquiry

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Yield:-

Steps:

Multi-step reaction with 2 steps
1: sulfuric acid / 2 h / 50 °C / Inert atmosphere; Schlenk technique
2: potassium carbonate / N,N-dimethyl-formamide / 2 h / 70 °C / Inert atmosphere; Schlenk technique

References:

Chen, Kai;Wu, Feng;Ye, Lijuan;Tian, Zi-You;Yu, Zhi-Xiang;Zhu, Shifa [Journal of Organic Chemistry,2016,vol. 81,# 18,p. 8155 - 8168]