ChemicalBook CAS DataBase List 4-Chloro-7,8,10,11,13,14-hexahydro-[1,4,7,10]tetraoxacyclododecino[2,3-g]quinazoline

4-Chloro-7,8,10,11,13,14-hexahydro-[1,4,7,10]tetraoxacyclododecino[2,3-g]quinazoline synthesis

9synthesis methods

Product Name:4-Chloro-7,8,10,11,13,14-hexahydro-[1,4,7,10]tetraoxacyclododecino[2,3-g]quinazoline
CAS Number:1204313-58-5
Molecular formula:C14H15ClN2O4
Molecular Weight:310.73

112-27-6 Synthesis

112-27-6
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4-Chloro-7,8,10,11,13,14-hexahydro-[1,4,7,10]tetraoxacyclododecino[2,3-g]quinazoline

1204313-58-5
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Yield:-

Steps:

Multi-step reaction with 6 steps
1: potassium hydroxide / dichloromethane / 8 h / Cooling with ice
2: potassium carbonate / N,N-dimethyl-formamide / 2 h / 120 °C
3: nitric acid; acetic acid / 24.5 h / 20 °C / Cooling with ice
4: palladium 10% on activated carbon; hydrogen / methanol / 13 h
5: formamide / 4 h / 165 °C
6: trichlorophosphate / 6 h / 110 °C

References:

Beijing Normal University;Qi, Chuanmin;Ren, Hongyu;Ning, Hongyu;Chang, Jin;Zhao, Mingxia;Chong, Yan;He, Yong CN105384745, 2016, A

1,4,7,10-Benzotetraoxacyclododecin-12-carboxylic acid, 2,3,5,6,8,9-hexahydro-, ethyl este

180475-66-5
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1204313-58-5
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References

Tri(Ethylene Glycol) DI-P-Toluenesulfonate

19249-03-7
220 suppliers
$9.00/1g

1204313-58-5
21 suppliers
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References

7,8,10,11,13,14-Hexahydro-[1,4,7,10]tetraoxacyclododecino[2,3-g]quinazolin-4(3H)-one

1204313-57-4
6 suppliers
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1204313-58-5
21 suppliers
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References

3943-89-3 Synthesis

3943-89-3
417 suppliers
$6.00/5g

1204313-58-5
21 suppliers
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References