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ChemicalBook CAS DataBase List 2-(4'-Piperidinyl) pyridine

2-(4'-Piperidinyl) pyridine synthesis

10synthesis methods
-

Yield:30532-37-7 88%

Reaction Conditions:

with hydrogen;10% Pd/C at 50; under 3102.97 Torr; for 40 h;

Steps:

36C EXAMPLE 36C; 2-(4-piperidinyl)pyridine

The product from Example 36B was treated with 10% Pd/C (250 mg) at 60 psi and 50° C. for 40 hours to provide the title compound (150 mg, 88% yield). MS (DCI/NH3) m/e 163 (M+H)+.

References:

US2003/229094,2003,A1 Location in patent:Page 73

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