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ChemicalBook CAS DataBase List 2,5,5-Trimethyl-1,3,2-dioxaphosphorinane 2-oxide

2,5,5-Trimethyl-1,3,2-dioxaphosphorinane 2-oxide synthesis

8synthesis methods
1005-69-2 Synthesis
2-methoxy-5,5-dimethyl-1,3,2-dioxaphosphorinane

1005-69-2
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Yield:873-97-2 99%

Reaction Conditions:

with trimethylsilyl bromide at 80;Inert atmosphere;

References:

Dabkowski, Wojciech;Ozarek, Alfred;Olejniczak, Sebastian;Cypryk, Marek;Chojnowski, Julian;Michalski, Jan [Chemistry - A European Journal,2009,vol. 15,# 7,p. 1747 - 1756] Location in patent:experimental part