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2,5-BIS(HEXYL)-1,4-BENZENEBIS(BORONIC ACID) synthesis

1synthesis methods
Benzene, 1,4-dihexyl-2,5-diiodo-

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2,5-BIS(HEXYL)-1,4-BENZENEBIS(BORONIC ACID)

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Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: n-BuLi / hexane / 12 h / 20 °C
1.2: hexane / -78 - 20 °C
2.1: 0.2250 g / aq. HCl / hexane / 3 h

References:

Niu, Weijun;Rambo, Brett;Smith, Mark D.;Lavigne, John J. [Chemical Communications,2005,# 41,p. 5166 - 5168]

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