![](/CAS/GIF/1883-75-6.gif)
2,5-Furandimethanol synthesis
- Product Name:2,5-Furandimethanol
- CAS Number:1883-75-6
- Molecular formula:C6H8O3
- Molecular Weight:128.13
![5-Hydroxymethylfurfural](/CAS/GIF/67-47-0.gif)
67-47-0
581 suppliers
$5.00/100mg
![2,5-Furandimethanol](/CAS/GIF/1883-75-6.gif)
1883-75-6
272 suppliers
$8.00/250mg
Yield:1883-75-6 100%
Reaction Conditions:
with hydrogen;3mol% Pt/C in ethanol at 20; under 3750.38 Torr; for 48 h;Product distribution / selectivity;
Steps:
4
Example 4.; Batch experiment with hydrogenation/etherification of 5- ( hy d roxy methyl )f u rf u ra I In a 7.5 ml batch reactor, 0.06 mmol 5-(hydroxymethyl)furfural (HMF) in 1 mL ethanol and 5 bars of hydrogen was reacted with 3 mol% of a Pt/C catalyst for 2 days at room temperature. The starting material was completely converted in 100% selectivity to 2,5- di(hydroxymethyl)furan. Subsequently, the mixture was heated to 75 0C for 1 day without hydrogen. The 2,5-di(hydroxymethyl)furan was fully converted and 2,5- bis(ethoxymethyl)furan was obtained in 75% yield. 25% Side products are ring opened levulinate derivatives. The experiment was successfully repeated on a 20 gram scale.
References:
WO2009/30509,2009,A2 Location in patent:Page/Page column 11
![5-Hydroxymethylfurfural](/CAS/GIF/67-47-0.gif)
67-47-0
581 suppliers
$5.00/100mg
![2,5-Furandimethanol](/CAS/GIF/1883-75-6.gif)
1883-75-6
272 suppliers
$8.00/250mg
![(5-(aminomethyl)furan-2-yl)methanol](/CAS/GIF/88910-22-9.gif)
88910-22-9
16 suppliers
$126.00/100mg
![5-Hydroxymethylfurfural](/CAS/GIF/67-47-0.gif)
67-47-0
581 suppliers
$5.00/100mg
![5-Methyl furfural](/CAS/GIF/620-02-0.gif)
620-02-0
478 suppliers
$14.14/5gm:
![2,5-Furandimethanol](/CAS/GIF/1883-75-6.gif)
1883-75-6
272 suppliers
$8.00/250mg
![Furfuryl alcohol](/CAS/GIF/98-00-0.gif)
98-00-0
457 suppliers
$23.00/50g
![Formaldehyde](/CAS/GIF/50-00-0.gif)
50-00-0
849 suppliers
$10.00/25g
![2,5-Furandimethanol](/CAS/GIF/1883-75-6.gif)
1883-75-6
272 suppliers
$8.00/250mg
![D(-)-Fructose](/CAS/20180808/GIF/57-48-7.gif)
57-48-7
550 suppliers
$12.00/250G
![2,5-Furandimethanol](/CAS/GIF/1883-75-6.gif)
1883-75-6
272 suppliers
$8.00/250mg