2-Benzylaminopyridine synthesis
- Product Name:2-Benzylaminopyridine
- CAS Number:6935-27-9
- Molecular formula:C12H12N2
- Molecular Weight:184.24
504-29-0
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$5.00/5 g
100-51-6
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$5.00/100g
6935-27-9
148 suppliers
$13.43/1gm:
Yield: 100%
Reaction Conditions:
with dichloro-[1,3-bis(4-tert-butylbenzyl)perhydrobenzimidazol-2-ylidene](p-cymene)ruthenium(II);potassium tert-butylate at 120; for 24 h;Inert atmosphere;Schlenk technique;Sealed tube;Reagent/catalyst;
Steps:
2.5. General procedure for the Nalkylation of amines with alcohols
General procedure: Under an inert atmosphere, KOBut (1 mmol), the aromatic amine (1 mmol), the alcohol derivative (1.5 mmol) and the Ru-NHC complex (2.5 mol%) were added to a Schlenk tube. The sealed Schlenk tube was stirred at 120 °C for 24 h. At the end of the reaction,the mixture was cooled to room temperature, CH2Cl2 (2 mL)was added and the resulting solution was filtered through a shortpad of SiO2. The filtrate was analysed by GC-MS with the calibrations based on dodecane.
References:
Yiğit, Beyhan;Özge Karaca, Emine;Yiğit, Murat;Gürbüz, Nevin;Arslan, Hakan;Özdemir, İsmail [Polyhedron,2020,vol. 175,art. no. 114234]
109-09-1
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100-46-9
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$5.00/5 g
6935-27-9
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$13.43/1gm:
109-04-6
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$6.00/25g
100-46-9
487 suppliers
$5.00/5 g
6935-27-9
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$13.43/1gm:
15009-91-3
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$11.00/250mg
100-51-6
1410 suppliers
$5.00/100g
6935-27-9
148 suppliers
$13.43/1gm:
504-29-0
552 suppliers
$5.00/5 g
100-52-7
962 suppliers
$17.30/2g
6935-27-9
148 suppliers
$13.43/1gm: