![](/CAS/GIF/117068-71-0.gif)
2-BROMO-6-BENZYLOXYPYRIDINE synthesis
- Product Name:2-BROMO-6-BENZYLOXYPYRIDINE
- CAS Number:117068-71-0
- Molecular formula:C12H10BrNO
- Molecular Weight:264.12
![2,6-Dibromopyridine](/CAS/GIF/626-05-1.gif)
626-05-1
497 suppliers
$9.00/10g
![Benzyl alcohol](/CAS/GIF/100-51-6.gif)
100-51-6
1378 suppliers
$5.00/100g
![2-BROMO-6-BENZYLOXYPYRIDINE](/CAS/GIF/117068-71-0.gif)
117068-71-0
75 suppliers
$55.00/250mg
Yield:117068-71-0 90%
Reaction Conditions:
Stage #1:benzyl alcohol with sodium hydride in tetrahydrofuran for 0.5 h;
Stage #2:2,6-Dibromopyridine in tetrahydrofuran at 20; for 18 h;
Steps:
20.1
Step l0.30 g (12 mmol) of sodium hydride was dispersed in anhydrous THF in a dried flask provided with nitrogen gas, benzylalcohol (12 mmol) was added thereto, and the mixture was stirred for 30 mins. After adding 2.4 g (10 mmol) of2,6-dibromopyridine thereto, the reaction mixture was kept at room temperature for 18 hrs, and the reaction was completed by adding water thereto. The resulting solution
References:
KOREA RESEARCH INSTITUTE OF CHEMICAL TECHNOLOGY;CHEMON INC. WO2008/153325, 2008, A1 Location in patent:Page/Page column 46-47
![2,6-Dibromopyridine](/CAS/GIF/626-05-1.gif)
626-05-1
497 suppliers
$9.00/10g
![SODIUM BENZYLOXIDE](/CAS/GIF/20194-18-7.gif)
20194-18-7
27 suppliers
$117.00/25ml
![2-BROMO-6-BENZYLOXYPYRIDINE](/CAS/GIF/117068-71-0.gif)
117068-71-0
75 suppliers
$55.00/250mg
![2-Bromo-6-hydroxypyridine](/CAS/GIF/27992-32-1.gif)
27992-32-1
172 suppliers
$9.00/250mg
![Benzyl bromide](/CAS/GIF/100-39-0.gif)
100-39-0
425 suppliers
$10.00/10 g
![2-BROMO-6-BENZYLOXYPYRIDINE](/CAS/GIF/117068-71-0.gif)
117068-71-0
75 suppliers
$55.00/250mg