ChemicalBook CAS DataBase List 2-PHENYL-2-PENTANOL

2-PHENYL-2-PENTANOL synthesis

12synthesis methods

Product Name:2-PHENYL-2-PENTANOL
CAS Number:4383-18-0
Molecular formula:C11H16O
Molecular Weight:164.24

4743-74-2
48 suppliers
$27.89/5g

4383-18-0
21 suppliers
$23.00/1g

Yield:4383-18-0 88%

Reaction Conditions:

with palladium diacetate;4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane in dichloromethane at 25; for 12 h;Schlenk technique;Inert atmosphere;

Steps:

11
Replace the gas environment in the Shrek tube with a nitrogen environment, add 2-phenyl-4-penten-2-ol 0.25 mmol, palladium acetate 0.00125 mmol, methylene chloride 0.5 mL, and add pinacol borane 0.275 with stirring mmol, reaction at room temperature for 12 h. The reaction solution obtained after the reaction was completed was subjected to column chromatography, and the target product obtained in 88% yield was a colorless liquid.

References:

Zhengzhou University;Cui Xiuling;Wang Yong;Pi Chao;Wu Yangjie CN111099986, 2020, A Location in patent:Paragraph 0034; 0085-0088

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108-86-1 Synthesis