2-VINYL-BENZOIC ACID ETHYL ESTER synthesis
- Product Name:2-VINYL-BENZOIC ACID ETHYL ESTER
- CAS Number:32082-32-9
- Molecular formula:C11H12O2
- Molecular Weight:176.21
2554-06-5
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6091-64-1
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32082-32-9
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$45.00/10mg
Yield:32082-32-9 99%
Reaction Conditions:
Stage #1: 2,4,6,8-tetramethyl-2,4,6,8-tetravinyl-cyclotetrasiloxanewith tetrabutyl ammonium fluoride;palladium(II) bromide;johnphos in tetrahydrofuran; for 0.166667 h;Inert atmosphere;Hiyama Amino-Acrylate Synthesis;
Stage #2: 2-bromobenzoic acid ethyl ester in tetrahydrofuran at 50; for 8 h;Inert atmosphere;
References:
Heberlig, Graham W.;Wirz, Monica;Wang, Meng;Boddy, Christopher N. [Organic Letters,2014,vol. 16,# 22,p. 5858 - 5861] Location in patent:supporting information
6091-64-1
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7486-35-3
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32082-32-9
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$45.00/10mg
64-17-5
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27326-43-8
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$68.09/100mg
32082-32-9
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$45.00/10mg
78-08-0
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$11.19/100G
1829-28-3
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32082-32-9
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$45.00/10mg
6091-64-1
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$10.00/1g
75927-49-0
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32082-32-9
22 suppliers
$45.00/10mg