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ChemicalBook CAS DataBase List 3-[9-(((3-(carboxypropyl)[4-Methxylphenyl]sulfonyl)aMine)carboxyl]-10-acridiniuMyl)-1-propanesulfonate inner salt
211106-69-3

3-[9-(((3-(carboxypropyl)[4-Methxylphenyl]sulfonyl)aMine)carboxyl]-10-acridiniuMyl)-1-propanesulfonate inner salt synthesis

3synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 4 steps
1: triethylamine / dichloromethane / 1 h / 20 °C
2: sodium hydride / dichloromethane / 7 h / 20 °C / Inert atmosphere
3: 1-methyl-pyrrolidin-2-one / 26 h / 125 °C / Inert atmosphere
4: hydrogenchloride / 16 h / 80 °C / Inert atmosphere

References:

CN111170994,2020,A

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