DIETHYL 2-ACETAMIDO-2-(BENZO(B)THIOPHENE-3-YLMETHYL)MALONATE synthesis
- Product Name:DIETHYL 2-ACETAMIDO-2-(BENZO(B)THIOPHENE-3-YLMETHYL)MALONATE
- CAS Number:23906-20-9
- Molecular formula:C18H21NO5S
- Molecular Weight:363.43
3216-47-5
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1068-90-2
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23906-20-9
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Yield:23906-20-9 80%
Reaction Conditions:
Stage #1: 2-acetylaminomalonic acid diethyl esterwith sodium hydride in N,N-dimethyl-formamide at 20; for 0.5 h;
Stage #2: 3-chloromethylbenzothiophene in N,N-dimethyl-formamide at 20 - 60; for 7 h;Further stages.;
References:
Paizs, Csaba;Katona, Adrian;Retey, Janos [Chemistry - A European Journal,2006,vol. 12,# 10,p. 2739 - 2744]
95-15-8
369 suppliers
$6.00/5g
23906-20-9
14 suppliers
$28.60/50MG