3-(2-Hydroxyphenyl)oxetan-3-ol synthesis
- Product Name:3-(2-Hydroxyphenyl)oxetan-3-ol
- CAS Number:1123786-87-7
- Molecular formula:C9H10O3
- Molecular Weight:166.17
Yield:1123786-87-7 75%
Reaction Conditions:
Stage #1: 2-hydroxybromobenzenewith n-butyllithium in diethyl ether;hexane at 20; for 0.5 h;Inert atmosphere;
Stage #2: oxetan-3-one in diethyl ether at 20; for 12 h;Inert atmosphere;
References:
White, Alexander R.;Kozlowski, Ryan A.;Tsai, Shiou-Chuan;Vanderwal, Christopher D. [Angewandte Chemie - International Edition,2017,vol. 56,# 35,p. 10525 - 10529][Angew. Chem.,2017,vol. 129,p. 10661 - 10665,5] Location in patent:supporting information
1123787-70-1
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