![](/CAS/GIF/2243-73-4.gif)
3-NITROBENZANILIDE synthesis
- Product Name:3-NITROBENZANILIDE
- CAS Number:2243-73-4
- Molecular formula:C13H10N2O3
- Molecular Weight:242.23
![1-Iodo-3-nitrobenzene](/CAS/GIF/645-00-1.gif)
645-00-1
9 suppliers
$50.00/1g
201230-82-2
1 suppliers
inquiry
![Aniline](/CAS/GIF/62-53-3.gif)
62-53-3
636 suppliers
$10.00/1g
![3-NITROBENZANILIDE](/CAS/GIF/2243-73-4.gif)
2243-73-4
23 suppliers
$60.00/500mg
Yield:2243-73-4 100%
Reaction Conditions:
with triethylamine in N,N-dimethyl-formamide at 100; under 750.075 Torr; for 8 h;Schlenk technique;Inert atmosphere;
Steps:
2.3.2. Catalytic reactions at atmospheric pressure
General procedure: In a typical experiment a solution containing the palladiumcatalyst (with 6 mol Pd-content) was placed in a Schlenk-tube.Under argon, 0.2 mmol (22.5 l) iodobenzene (1), 0.5 mmol aminereagent, 0.7 mmol (100 l) triethylamine and 1 ml solvent wasadded and the atmosphere was changed to carbon monoxide. Thereaction mixture was heated with stirring in an oil bath at 100Cand was analysed by gas chromatography.
References:
Urbán, Béla;Papp, Máté;Srankó, Dávid;Skoda-F?ldes, Rita [Journal of Molecular Catalysis A: Chemical,2015,vol. 397,p. 150 - 157]
![Aniline](/CAS/GIF/62-53-3.gif)
62-53-3
636 suppliers
$10.00/1g
![3-Nitrobenzoic acid](/CAS/GIF/121-92-6.gif)
121-92-6
553 suppliers
$6.00/25g
![3-NITROBENZANILIDE](/CAS/GIF/2243-73-4.gif)
2243-73-4
23 suppliers
$60.00/500mg
![Iodobenzene](/CAS/GIF/591-50-4.gif)
591-50-4
473 suppliers
$10.00/1g
![3-NITROBENZAMIDE](/CAS/GIF/645-09-0.gif)
645-09-0
112 suppliers
$18.89/10g
![3-NITROBENZANILIDE](/CAS/GIF/2243-73-4.gif)
2243-73-4
23 suppliers
$60.00/500mg
![m-Nitrobenzoyl chloride](/CAS/GIF/121-90-4.gif)
121-90-4
5 suppliers
$24.00/25g
![3-NITROBENZANILIDE](/CAS/GIF/2243-73-4.gif)
2243-73-4
23 suppliers
$60.00/500mg