Propanedioic acid, 2-methyl-2-(phenylmethoxy)-, 1,3-dimethyl ester synthesis
- Product Name:Propanedioic acid, 2-methyl-2-(phenylmethoxy)-, 1,3-dimethyl ester
- CAS Number:344798-16-9
- Molecular formula:C13H16O5
- Molecular Weight:252.26
31600-43-8
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Yield:-
Steps:
Multi-step reaction with 2 steps
1: 59 percent / LDA / tetrahydrofuran; hexane / -78 °C
2: 69 percent / t-BuOLi / 2-methyl-propan-2-ol; hexane / 6 h / 20 °C
References:
Guanti, Giuseppe;Banfi, Luca;Powles, Katharine;Rasparini, Marcello;Scolastico, Carlo;Fossati, Novella [Tetrahedron Asymmetry,2001,vol. 12,# 2,p. 271 - 277]
