![](/CAS/20211123/GIF/39729-00-5.gif)
Benzeneacetic acid, 4-methoxy-α-methylene-, ethyl ester synthesis
- Product Name:Benzeneacetic acid, 4-methoxy-α-methylene-, ethyl ester
- CAS Number:39729-00-5
- Molecular formula:C12H14O3
- Molecular Weight:206.24
Yield:39729-00-5 98%
Reaction Conditions:
Stage #1: 2-bromo-acrylic acid ethyl esterwith naphthalene;tetraethylammonium perchlorate;zinc in N,N-dimethyl-formamide at -20; for 1 h;
Stage #2: para-iodoanisole;dichlorobis(tri-O-tolylphosphine)palladium in N,N-dimethyl-formamide at 70; for 3 h;
References:
Jalil;Kurono;Tokuda [Synlett,2001,# 12,p. 1944 - 1946]
![ETHYL 4-METHOXYBENZOYLFORMATE](/CAS/GIF/40140-16-7.gif)
40140-16-7
70 suppliers
$15.00/250mg
![Methyltriphenylphosphonium bromide](/CAS/GIF/1779-49-3.gif)
1779-49-3
591 suppliers
$5.00/10g
![Benzeneacetic acid, 4-methoxy-α-methylene-, ethyl ester](/CAS/20211123/GIF/39729-00-5.gif)
39729-00-5
1 suppliers
inquiry
![ETHYL 2-BROMOACRYLATE](/CAS/GIF/5459-35-8.gif)
5459-35-8
48 suppliers
$175.00/500mg
![4-Methoxyphenylboronic acid](/CAS/GIF/5720-07-0.gif)
5720-07-0
454 suppliers
$6.00/5g
![Benzeneacetic acid, 4-methoxy-α-methylene-, ethyl ester](/CAS/20211123/GIF/39729-00-5.gif)
39729-00-5
1 suppliers
inquiry