ChemicalBook CAS DataBase List 4-BROMO-2,3-DIHYDRO-1H-INDEN-1-OL

4-BROMO-2,3-DIHYDRO-1H-INDEN-1-OL synthesis

8synthesis methods

Product Name:4-BROMO-2,3-DIHYDRO-1H-INDEN-1-OL
CAS Number:16657-10-6
Molecular formula:C9H9BrO
Molecular Weight:213.07

3433-80-5 Synthesis

3433-80-5
315 suppliers
$10.00/1g

16657-10-6
66 suppliers
$25.00/250mg

Yield:-

Steps:

Multi-step reaction with 6 steps
1: 64 percent / NaOC₂H₅ / 3.5 h / Heating
2: 89 percent / KOH / acetic acid; H₂O; tetrahydrofuran / 12 h / 25 °C
3: 81 percent / 165 °C
4: thionyl chloride / 0.75 h / Heating
5: 93 percent / AlCl₃ / CS₂ / 3 h / Heating
6: 98 percent / NaBH₄ / ethanol / 2 h / 25 °C

References:

Adamczyk, Maciej;Watt, David S.;Netzel, Daniel A. [Journal of Organic Chemistry,1984,vol. 49,# 22,p. 4226 - 4237]

15115-60-3 Synthesis