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5734-62-3

4-chloro-N,N,6-trimethylpyrimidin-2-amine synthesis

3synthesis methods
-

Yield:5734-62-3 74 mg

Reaction Conditions:

Stage #1: 2-amino-6-methyl-4-chloropyrimidinewith sodium hydride in tetrahydrofuran at 0 - 20; for 0.0833333 h;
Stage #2: methyl iodide in tetrahydrofuran at 20; for 16 h;

References:

Henderson, Scott H.;Sorrell, Fiona;Bennett, James;Fedorov, Oleg;Hanley, Marcus T.;Godoi, Paulo H.;Ruela De Sousa, Roberta;Robinson, Sean;Ashall-Kelly, Alexander;Hopkins Navratilova, Iva;Walter, Daryl S.;Elkins, Jonathan M.;Ward, Simon E. [Journal of Medicinal Chemistry,2021,vol. 64,# 15,p. 11709 - 11728] Location in patent:supporting information

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