4-Quinolinol, decahydro- synthesis
- Product Name:4-Quinolinol, decahydro-
- CAS Number:49788-04-7
- Molecular formula:C9H17NO
- Molecular Weight:155.24
58869-89-9
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Yield:49788-04-7 96.8%
Reaction Conditions:
with sodium tetrahydroborate in tetrahydrofuran at 0; for 2 h;
Steps:
4.1 1. Preparation of decahydroquinolin-4-ol
Octahydroquinoline-4 (1H)-one (500 mg, 3.3 mmol) was added to THF (10 mL), and sodium borohydride (250 mg, 6.6 mmol) was added at 0 °C for 2 hours. Add 40 mL of water and ethyl acetate to extract.The organic phase is concentrated to give the title compound(496 mg, yield: 96.8%).
References:
CN109575008,2019,A Location in patent:Paragraph 0278; 0280; 0281; 0282
36940-67-7
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