![](/CAS/GIF/54464-14-1.gif)
5-(4-Methoxyphenyl)-4H-1,2,4-triazol-3-amine synthesis
- Product Name:5-(4-Methoxyphenyl)-4H-1,2,4-triazol-3-amine
- CAS Number:54464-14-1
- Molecular formula:C9H10N4O
- Molecular Weight:190.2
![Cyanamide](/CAS/GIF/420-04-2.gif)
420-04-2
339 suppliers
$15.00/25g
![Anisonitrile](/CAS/GIF/874-90-8.gif)
874-90-8
344 suppliers
$8.00/10g
![5-(4-Methoxyphenyl)-4H-1,2,4-triazol-3-amine](/CAS/GIF/54464-14-1.gif)
54464-14-1
29 suppliers
$98.00/1g
Yield:54464-14-1 92%
Reaction Conditions:
Stage #1: CYANAMIDwith hydroxylamine hydrochloride;triethylamine in ethanol at 100; for 12 h;Inert atmosphere;Schlenk technique;
Stage #2: 4-methoxybenzonitrilewith iron(III) chloride;potassium carbonate in ethanol;dimethyl sulfoxide at 100; for 12 h;Sealed tube;Inert atmosphere;Schlenk technique;
References:
Rohand, Taoufik;Mkpenie, Victor N.;El Haddad, Mohammadine;Markó, István E. [Journal of Heterocyclic Chemistry,2019,vol. 56,# 2,p. 690 - 695]
![4-Methoxybenzoyl chloride](/CAS/GIF/100-07-2.gif)
100-07-2
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$35.00/25g
![5-(4-Methoxyphenyl)-4H-1,2,4-triazol-3-amine](/CAS/GIF/54464-14-1.gif)
54464-14-1
29 suppliers
$98.00/1g
![4-Methoxybenzoic acid](/CAS/GIF/100-09-4.gif)
100-09-4
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$6.00/25g
![5-(4-Methoxyphenyl)-4H-1,2,4-triazol-3-amine](/CAS/GIF/54464-14-1.gif)
54464-14-1
29 suppliers
$98.00/1g
![Methyl anisate](/CAS/GIF/121-98-2.gif)
121-98-2
280 suppliers
$12.00/1mg
![5-(4-Methoxyphenyl)-4H-1,2,4-triazol-3-amine](/CAS/GIF/54464-14-1.gif)
54464-14-1
29 suppliers
$98.00/1g