5-Benzo[1,3]dioxol-5-yl-3,4-dihydro-2H-pyrrole synthesis

4synthesis methods

Product Name:5-Benzo[1,3]dioxol-5-yl-3,4-dihydro-2H-pyrrole
CAS Number:95849-35-7
Molecular formula:C11H11NO2
Molecular Weight:189.21

Pentanedinitrile, 2-(1,3-benzodioxol-5-yl)-2-(4-morpholinyl)-

95877-46-6
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5-Benzo[1,3]dioxol-5-yl-3,4-dihydro-2H-pyrrole

95849-35-7
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: 97 percent / glacial CH₃COOH, H₂O / tetrahydrofuran / 18 h / 70 °C
2: 90 percent / H₂ / Raney Ni / methanol / 8 h / 100 °C

References:

Dallacker;Jouck [Zeitschrift fur Naturforschung, Teil B: Anorganische Chemie, Organische Chemie,1984,vol. 39,# 11,p. 1598 - 1606]

1,3-Benzodioxole-5-butanenitrile, γ-oxo-

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References

2-(1,3-BENZODIOXOL-5-YL)-2-MORPHOLINOACETONITRILE

37673-10-2
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95849-35-7
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References

2635-13-4 Synthesis

2635-13-4
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References

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