ChemicalBook CAS DataBase List 5-bromo-3-methyl-2-(methylthio)pyrimidin-4(3H)-one

5-bromo-3-methyl-2-(methylthio)pyrimidin-4(3H)-one synthesis

6synthesis methods

Product Name:5-bromo-3-methyl-2-(methylthio)pyrimidin-4(3H)-one
CAS Number:81560-06-7
Molecular formula:C6H7BrN2OS
Molecular Weight:235.1

6327-98-6 Synthesis

2-(Methylthio)-3-methylpyrimidine-4(3H)-one

6327-98-6
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5-bromo-3-methyl-2-(methylthio)pyrimidin-4(3H)-one

81560-06-7
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Yield:81560-06-7 100%

Reaction Conditions:

with bromine in chloroform at 0; for 0.583333 h;Inert atmosphere;

References:

D'Angelo, Noel D.;Bellon, Steven F.;Booker, Shon K.;Cheng, Yuan;Coxon, Angela;Dominguez, Celia;Fellows, Ingrid;Hoffman, Douglas;Hungate, Randall;Kaplan-Lefko, Paula;Lee, Matthew R.;Li, Chun;Liu, Longbin;Rainbeau, Elizabeth;Reider, Paul J.;Rex, Karen;Siegmund, Aaron;Sun, Yaxiong;Tasker, Andrew S.;Xi, Ning;Xu, Shimin;Yang, Yajing;Zhang, Yihong;Burgess, Teresa L.;Dussault, Isabelle;Kim, Tae-Seong [Journal of Medicinal Chemistry,2008,vol. 51,# 18,p. 5766 - 5779] Location in patent:experimental part

81560-03-4 Synthesis