5-CHLORO-1-METHYLINDOLIN-2-ONE synthesis
- Product Name:5-CHLORO-1-METHYLINDOLIN-2-ONE
- CAS Number:41192-33-0
- Molecular formula:C9H8ClNO
- Molecular Weight:181.62
Yield:41192-33-0 86%
Reaction Conditions:
Stage #1: 5-chloroindole 2,3-dione;methyl iodidewith sodium hydride in N,N-dimethyl-formamide at 0;
Stage #2: with hydrazineReflux;
References:
Sattar, Moh.;Rathore, Vandana;Prasad, Ch. Durga;Kumar, Sangit [Chemistry - An Asian Journal,2017,vol. 12,# 7,p. 734 - 743] Location in patent:supporting information
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