5-Chloropyridine-2-thiol synthesis
- Product Name:5-Chloropyridine-2-thiol
- CAS Number:40771-41-3
- Molecular formula:C5H4ClNS
- Molecular Weight:145.61
16110-09-1
454 suppliers
$5.00/1g
40771-41-3
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$45.00/100mg
Yield: 47%
Reaction Conditions:
Stage #1:2,5 dichloropyridine with thiourea in ethanol at 95; for 22 h;
Stage #2: with potassium hydroxide in water at 95; for 2 h;
References:
Liu, Ping;Hamill, Terence G.;Chioda, Marc;Chobanian, Harry;Fung, Selena;Guo, Yan;Chang, Linda;Bakshi, Raman;Hong, Qingmei;Dellureficio, James;Lin, Linus S.;Abbadie, Catherine;Alexander, Jessica;Jin, Hong;Mandala, Suzanne;Shiao, Lin-Lin;Li, Wenping;Sanabria, Sandra;Williams, David;Zeng, Zhizhen;Hajdu, Richard;Jochnowitz, Nina;Rosenbach, Mark;Karanam, Bindhu;Madeira, Maria;Salituro, Gino;Powell, Joyce;Xu, Ling;Terebetski, Jenna L.;Leone, Joseph F.;Miller, Patricia;Cook, Jacquelynn;Holahan, Marie;Joshi, Aniket;O'Malley, Stacey;Purcell, Mona;Posavecz, Diane;Chen, Tsing-Bau;Riffel, Kerry;Williams, Mangay;Hargreaves, Richard;Sullivan, Kathleen A.;Nargund, Ravi P.;DeVita, Robert J. [ACS Medicinal Chemistry Letters,2013,vol. 4,# 6,p. 509 - 513] Location in patent:supporting information
1480-65-5
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$7.00/1g
40771-41-3
64 suppliers
$45.00/100mg
4214-79-3
240 suppliers
$6.00/1g
40771-41-3
64 suppliers
$45.00/100mg