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ChemicalBook CAS DataBase List 6-Aminofluorescein

6-Aminofluorescein synthesis

5synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: 200 °C
1.2: 2 h / Reflux
2.1: sodium hydroxide / methanol / Heating
3.1: sodium sulfide nonahydrate; sodium hydrogensulfide / water / 24 h / Reflux

References:

Tomasch, Miriam;Schwed, J. Stephan;Kuczka, Karina;Meyer Dos Santos, Sascha;Harder, Sebastian;Nuesing, Rolf M.;Paulke, Alexander;Stark, Holger [ACS Medicinal Chemistry Letters,2012,vol. 3,# 9,p. 774 - 779]

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