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ChemicalBook CAS DataBase List 3-[(Aminoiminomethyl)amino]-4-methylbenzoic acid ethyl ester mononitrate

3-[(Aminoiminomethyl)amino]-4-methylbenzoic acid ethyl ester mononitrate synthesis

6synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: sulfuric acid / 12 h / Reflux; Inert atmosphere
2: hydrogenchloride / ethanol; water / 15 h / Reflux
3: ammonium nitrate / 0.5 h / 0 °C

References:

Pan, Xiaoyan;Dong, Jinyun;Gao, Hongping;Wang, Fang;Zhang, Yanmin;Wang, Sicen;Zhang, Jie [Chemical Biology and Drug Design,2014,vol. 83,# 5,p. 592 - 599]

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