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7H-Pyrrolo[2,3-d]pyrimidine, 7-methyl- (9CI) synthesis

3synthesis methods
3680-71-5 Synthesis
Pyrrolo[2,3-d]pyrimidin-4-ol

3680-71-5
396 suppliers
$6.00/1g

7H-Pyrrolo[2,3-d]pyrimidine, 7-methyl- (9CI)

87791-29-5
4 suppliers
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: 80 percent / P4S10 / pyridine / 3 h / Heating
2: 69 percent / finely divided nickel / aq. NH3 / 0.5 h / Heating
3: 53 percent / (C4H9)4NHSO4, 50percent-NaOH / 1,2-dimethoxy-ethane; CH2Cl2

References:

Seela, Frank;Steker, Herbert [Liebigs Annalen der Chemie,1983,# 9,p. 1576 - 1587]