ChemicalBook CAS DataBase List methyl 5-(aminomethyl)-2-chlorobenzoate hydrochloride

methyl 5-(aminomethyl)-2-chlorobenzoate hydrochloride synthesis

4synthesis methods

Product Name:methyl 5-(aminomethyl)-2-chlorobenzoate hydrochloride
CAS Number:90942-47-5
Molecular formula:C9H11Cl2NO2
Molecular Weight:236.0951

118-91-2 Synthesis

118-91-2
640 suppliers
$8.50/5g

methyl 5-(aminomethyl)-2-chlorobenzoate hydrochloride

90942-47-5
62 suppliers
$143.00/1g

Yield:-

Steps:

Multi-step reaction with 4 steps
1.1: sulfuric acid / 16 h / 22 - 26 °C
2.1: hydrogenchloride / water; 1,4-dioxane / 12 h / Reflux
2.2: 16 h / 0 - 26 °C
3.1: potassium carbonate / N,N-dimethyl-formamide / 18 h / 22 - 26 °C
4.1: hydrogenchloride / ethyl acetate / 2 h / 22 - 26 °C

References:

GLENMARK PHARMACEUTICALS S.A.;GHARAT, Laxmikant Atmaram;BANERJEE, Abhisek;KHAIRATKAR-JOSHI, Neelima;KATTIGE, Vidya Ganapati WO2013/72825, 2013, A1

FullText

1294496-57-3 Synthesis

Benzoic acid, 2-chloro-5-[[(2,2,2-trifluoroacetyl)amino]methyl]-

1294496-57-3
1 suppliers
inquiry

90942-47-5
62 suppliers
$143.00/1g

References

5-(BOC-AMINO)METHYL-2-CHLORO-BENZOIC ACID

165950-04-9
13 suppliers
inquiry

90942-47-5
62 suppliers
$143.00/1g

References

90434-27-8
11 suppliers
inquiry

90942-47-5
62 suppliers
$143.00/1g

References

methyl 5-(aminomethyl)-2-chlorobenzoate hydrochloride Related Search:

Benzoic acid, 5-(bromomethyl)-2-methoxy-, methyl ester