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ChemicalBook CAS DataBase List 3-(2-Chloroethyl)-6,7,8,9-tetrahydro-2-methyl-4H-pyrido[1,2-a]pyrimidin-4-one

3-(2-Chloroethyl)-6,7,8,9-tetrahydro-2-methyl-4H-pyrido[1,2-a]pyrimidin-4-one synthesis

5synthesis methods
1897-52-5 Synthesis
2,6-Difluorobenzonitrile

1897-52-5
520 suppliers
$7.00/10g

-

Yield:-

Steps:

Multi-step reaction with 4 steps
2: H2NOH*HCl, aq. KOH / propan-2-ol / 10 h / Heating
3: 43 percent / K2CO3 / CHCl3 / 4 h
4: LAH / tetrahydrofuran / 1.5 h / Heating

References:

Strupczewski, Joseph T.;Allen, Richard C.;Gardner, Beth Ann;Schmid, Blaine L.;Stache, Ulrich;et al. [Journal of Medicinal Chemistry,1985,vol. 28,# 6,p. 761 - 769]

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