ACIVICIN synthesis
- Product Name:ACIVICIN
- CAS Number:42228-92-2
- Molecular formula:C5H7ClN2O3
- Molecular Weight:178.57
56-86-0
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42228-92-2
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Yield:-
Steps:
Multi-step reaction with 9 steps
1: Cl2, H2SO4 / 5 h / Irradiation
2: 85 percent / pH 9
3: 85 percent / dicyclohexylcarbodiimide / ethyl acetate / 0 °C
4: tetrahydrofuran / -50 - -30 °C
5: hydroxylamine / H2O / pH 6
6: Et3N / H2O / Ambient temperature; pH 11
7: tetrahydrofuran
8: 54 percent / dichlorotris(dimethylamino)phosphorane / tetrahydrofuran / Heating
9: 87 percent / trifluoroacetic acid, thioanisole
References:
Silverman, Richard B.;Holladay, Mark W. [Journal of the American Chemical Society,1981,vol. 103,# 24,p. 7357 - 7358]
105834-88-6
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![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
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42228-92-2
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1000210-73-0
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42228-92-2
81 suppliers
$40.00/1mg
1000210-73-0
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42228-92-2
81 suppliers
$40.00/1mg