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ChemicalBook CAS DataBase List ACT-462206

ACT-462206 synthesis

9synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: triethylamine; chloroformic acid ethyl ester / dichloromethane / 1 h / 20 °C
2: hydrogenchloride / 1,4-dioxane / 1 h / 20 °C
3: N-ethyl-N,N-diisopropylamine / acetonitrile / 15 h / 20 °C

References:

Tortoioli, Simone;Marchal, Daniel;Kesselgruber, Martin;Pabst, Thomas;Skranc, Wolfgang;Abele, Stefan [Organic Process Research and Development,2014,vol. 18,# 12,p. 1759 - 1762]