Benzoic acid, 2,3,6-tribroMo- synthesis
- Product Name:Benzoic acid, 2,3,6-tribroMo-
- CAS Number:21739-99-1
- Molecular formula:C7H3Br3O2
- Molecular Weight:358.81
108-36-1
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21739-99-1
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Yield:-
Steps:
Multi-step reaction with 3 steps
1.1: diisopropylamine; BuLi / tetrahydrofuran; hexane / 2 h / -75 °C
1.2: 92 percent / tetrahydrofuran; hexane / -75 °C
2.1: 96 percent / Br2 / CCl4 / 96 h / Heating
3.1: BuLi; N-tert-butyl-N-(tert-butyldimethylsilyl)amine / tetrahydrofuran / -75 °C
3.2: 50 percent / tetrahydrofuran / -75 °C
References:
Mongin, Florence;Marzi, Elena;Schlosser, Manfred [European Journal of Organic Chemistry,2001,# 14,p. 2771 - 2777]
124-38-9
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608-21-9
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363598-42-9
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124-38-9
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615-54-3
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633-12-5
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21739-99-1
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124-38-9
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608-21-9
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601-84-3
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87976-24-7
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21739-99-1
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87976-25-8
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