![](/CAS/GIF/4613-78-9.gif)
BETA-GENTIOBIOSE OCTAACETATE synthesis
- Product Name:BETA-GENTIOBIOSE OCTAACETATE
- CAS Number:4613-78-9
- Molecular formula:C28H38O19
- Molecular Weight:678.59
![2,3,4,6-TETRA-O-ACETYL-ALPHA-D-GLUCOPYRANOSYL TRICHLOROACETIMIDATE](/CAS/GIF/74808-10-9.gif)
74808-10-9
47 suppliers
$60.00/25mg
![2,3,4,6-TETRA-O-ACETYL-BETA-D-GLUCOPYRANOSE](/CAS/GIF/13100-46-4.gif)
13100-46-4
116 suppliers
$68.29/1g
![BETA-GENTIOBIOSE OCTAACETATE](/CAS/GIF/4613-78-9.gif)
4613-78-9
32 suppliers
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Yield:4613-78-9 43%
Reaction Conditions:
Stage #1: O-(2,3,4,6-Tetra-O-acetyl-α-D-glucopyranosyl)trichloroacetimidate;1,2,3,4-tetra-O-acetyl-β-D-glucopyranose in dichloromethane at 20; for 1 h;Inert atmosphere;Molecular sieve;
Stage #2: with trimethylsilyl trifluoromethanesulfonate in dichloromethane at -40; for 16 h;Inert atmosphere;Molecular sieve;diastereoselective reaction;
References:
Weber, Julia;Mikula, Hannes;Fruhmann, Philipp;Hametner, Christian;Varga, Elisabeth;Berthiller, Franz;Krska, Rudolf;Fr?hlich, Johannes [Synlett,2013,vol. 24,# 14,art. no. ST-2013-D0484-L,p. 1830 - 1834] Location in patent:supporting information
![2,3,4,6-TETRA-O-ACETYL-BETA-D-GLUCOPYRANOSE](/CAS/GIF/13100-46-4.gif)
13100-46-4
116 suppliers
$68.29/1g
![BETA-GENTIOBIOSE OCTAACETATE](/CAS/GIF/4613-78-9.gif)
4613-78-9
32 suppliers
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![Acetic anhydride](/CAS/20180808/GIF/108-24-7.gif)
108-24-7
5 suppliers
$14.00/250ML
![GENTIOBIOSE](/CAS/GIF/554-91-6.gif)
554-91-6
188 suppliers
$44.79/250MG
![BETA-GENTIOBIOSE OCTAACETATE](/CAS/GIF/4613-78-9.gif)
4613-78-9
32 suppliers
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![6-TRITYL-1,2,3,4-TETRA-O-ACETYL-BETA-D-GLUCOSE](/CAS/GIF/37074-90-1.gif)
37074-90-1
51 suppliers
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![BETA-GENTIOBIOSE OCTAACETATE](/CAS/GIF/4613-78-9.gif)
4613-78-9
32 suppliers
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