Diacetyl-L-Glycerophosphorylcholine synthesis
- Product Name:Diacetyl-L-Glycerophosphorylcholine
- CAS Number:54672-38-7
- Molecular formula:C12H24NO8P
- Molecular Weight:341.2946
Yield:54672-38-7 76%
Reaction Conditions:
Stage #1: (S)-1,2-O-Diacetylglycerolwith triethylamine;trichlorophosphate in dichloromethane at 0; for 0.833333 h;
Stage #2: choline tosylatewith pyridine in dichloromethane at 20; for 12 h;Inert atmosphere;
Stage #3: with water in dichloromethane; for 1 h;
References:
Park, Jong Moon;De Castro, Kathlia A.;Ahn, Hyunseok;Rhee, Hakjune [Bulletin of the Korean Chemical Society,2010,vol. 31,# 9,p. 2689 - 2691] Location in patent:experimental part
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