Diallyl sulfide synthesis
- Product Name:Diallyl sulfide
- CAS Number:592-88-1
- Molecular formula:C6H10S
- Molecular Weight:114.21
14180-63-3
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592-88-1
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Yield:592-88-1 90%
Reaction Conditions:
with iodine;sodium hydrogensulfite in chloroform at 50; for 3 h;Temperature;
Steps:
General procedure:
General procedure: A mixture of a sulfoxide (1 mmol), NaHSO3 (1.1 mmol), and I2 (0.025-0.1 mmol) in CHCl3 (1 mL) was stirred at room temperature or at 50 °C. The progress of the reaction was monitored by TLC. After completion, the solution was decanted from the residue, washed with EtOAc (2 x 1 mL). The combined organic layers were concentrated and the residue purified by chromatography on silica gel using n-hexane as eluent.
References:
Abbasi, Mohammad;Mohammadizadeh, Mohammad Reza;Moradi, Zahra [Tetrahedron Letters,2015,vol. 56,# 47,p. 6610 - 6613]
107-05-1
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2179-57-9
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592-88-1
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2050-87-5
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$31.00/25mg
107-05-1
397 suppliers
$16.80/100ML
2179-57-9
359 suppliers
$6.00/5g
592-88-1
182 suppliers
$15.00/1g
2050-87-5
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$31.00/25mg
2444-49-7
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6329-40-4
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592-88-1
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538-74-9
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6937-97-9
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106-95-6
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592-88-1
182 suppliers
$15.00/1g