Indan-2-amine synthesis
- Product Name:Indan-2-amine
- CAS Number:2975-41-9
- Molecular formula:C9H11N
- Molecular Weight:133.19
615-13-4
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$8.00/5g
2975-41-9
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$48.50/1g
Yield:2975-41-9 93%
Reaction Conditions:
with palladium on activated charcoal;hydrogen;acetic acid;benzylamine in isopropyl alcohol at 80; under 22502.3 Torr;Autoclave;Solvent;Pressure;
Steps:
1-3 Example 3
In an autoclave, add 150g of 2-indanone, 145g of benzylamine, 600ml of isopropanol, and 8ml of glacial acetic acid. Add 20g of palladium-carbon catalyst, pass hydrogen to 3Mpa, and react at 80 ° C. After the reaction, press filter, concentrate the filtrate, and rectify 140 g of product were obtained, yield: 93%.
References:
Nanjing Huanran Biological Technology Co., Ltd.;Wang Kunpeng;Han Yuelin CN110229067, 2019, A Location in patent:Paragraph 0028-0033
17623-96-0
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175079-50-2
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95-13-6
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2975-41-9
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