![](/CAS/GIF/65373-53-7.gif)
ISOXAZOLE-4-CARBALDEHYDE synthesis
- Product Name:ISOXAZOLE-4-CARBALDEHYDE
- CAS Number:65373-53-7
- Molecular formula:C4H3NO2
- Molecular Weight:97.07
![4-HYDROXYMETHYL-ISOXAZOLE](/CAS/GIF/102790-36-3.gif)
102790-36-3
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65373-53-7
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$45.00/10mg
Yield: 20%
Reaction Conditions:
with Dess-Martin periodane in dichloromethane at 20;
Steps:
21e
Experiment 21; The intermediate 2, was prepared in 37% yield using the method as described in ref.: J. Org. Chem. 1982, 47, 2216-17. The ethyl ester 4 was prepared by the literature method (Ref: Gazz. CMm. Ital. 1947, 77, 206-12). Following lithium aluminium hydride reduction gave the alcohol 5 which was oxides to the aldehyde 6.
References:
AVEXA LIMITED WO2007/124546, 2007, A1 Location in patent:Page/Page column 61
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6455-40-9
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$45.00/25mg
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65373-53-7
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$45.00/10mg
![4-Isoxazolecarboxylic acid](/CAS/GIF/6436-62-0.gif)
6436-62-0
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$14.00/100mg
![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
1000210-73-0
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![ISOXAZOLE-4-CARBALDEHYDE](/CAS/GIF/65373-53-7.gif)
65373-53-7
53 suppliers
$45.00/10mg