ChemicalBook CAS DataBase List METHYL 1-METHYLPYRROLE-2-CARBOXYLATE

METHYL 1-METHYLPYRROLE-2-CARBOXYLATE synthesis

13synthesis methods

Product Name:METHYL 1-METHYLPYRROLE-2-CARBOXYLATE
CAS Number:37619-24-2
Molecular formula:C7H9NO2
Molecular Weight:139.15

67-56-1 Synthesis

67-56-1
737 suppliers
$7.29/5ml-f

6973-60-0
200 suppliers
$6.00/250mg

18107-18-1
204 suppliers
$33.00/5g

37619-24-2
105 suppliers
$10.00/500mg

Yield:-

Reaction Conditions:

at 20; for 1 h;

Steps:

26
To a solution of 1-methyl-2-pyrrolecarboxylic acid (1.03 g, 8.22 mmol) in MeOH (5 mL) and dioxane (5 mL) at room temperature, trimethylsilyldiazomethane (2M in ether, 5.0 mL, 10.0 mmol) was added. After being stirred at room temperature for 1 h, the mixture was concentrated in vacuo to give methyl 1-methyl-2-pyrrolecarboxylate as a volatile oil (1.14 g).

References:

Millennium Pharmaceuticals, Inc. US2007/259924, 2007, A1 Location in patent:Page/Page column 33

1193-62-0 Synthesis