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N,N-Diethyl-o-phenylenediamine synthesis

4synthesis methods
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Yield:19056-34-9 66 %

Reaction Conditions:

Stage #1: diethylamine;ortho-nitrofluorobenzenewith potassium carbonate in dimethyl sulfoxide at 110;
Stage #2: with iron;ammonium chloride in ethanol;water at 90;

References:

Yi, Xiaofei;Zhao, Zongxiang;Wang, Manman;Yu, Wenquan;Chang, Junbiao [Organic Letters,2022,vol. 24,# 47,p. 8703 - 8708] Location in patent:supporting information

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