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ChemicalBook CAS DataBase List N-NONYL-BETA-D-GLUCOPYRANOSIDE

N-NONYL-BETA-D-GLUCOPYRANOSIDE synthesis

8synthesis methods
-

Yield:69984-73-2 2.92%

Reaction Conditions:

with almond meal in water at 50; for 168 h;Thermodynamic data;Equilibrium constant;Enzymatic reaction;

Steps:

1.1 Enzymatic synthesis of alkyl β-D-glucosides
General procedure: In a typical experiment, an alkyl alcohol was used as thesubstrate and the medium. The reaction mixture was composedof 18 ml of primary alcohol and 2 ml of water containing 0.25mol/L glucose (Scheme 1). After 60 mg almond meal wasadded, the mixture was incubated in a 100-ml flask and constantlyshaken at 180 r/min at 50 °C. At certain intervals, 50 lof the mixture was withdrawn and analyzed by HPLC.For the synthesis of methyl -D-glucoside, 2 ml of methanol,16 ml of acetonitrile, and 2 ml of water containing 0.25 mol/Lglucose were mixed.

References:

Wang, Qinqqin;Yu, Huilei;Zhao, Na;Li, Chunxiu;Shang, Yazhuo;Liu, Honglai;Xu, Jianhe [Cuihua Xuebao/Chinese Journal of Catalysis,2012,vol. 33,# 2-3,p. 275 - 280]

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