![](/CAS/GIF/1864-94-4.gif)
PHENYL FORMATE synthesis
- Product Name:PHENYL FORMATE
- CAS Number:1864-94-4
- Molecular formula:C7H6O2
- Molecular Weight:122.12
![Formic acid](/CAS/GIF/64-18-6.gif)
64-18-6
1063 suppliers
$22.12/250ML
![Phenol](/CAS/20180808/GIF/108-95-2.gif)
108-95-2
725 suppliers
$14.00/25g
![PHENYL FORMATE](/CAS/GIF/1864-94-4.gif)
1864-94-4
89 suppliers
$6.00/1g
Yield:1864-94-4 98.4%
Reaction Conditions:
with toluene-4-sulfonic acid in toluene at 105; for 4 h;Reagent/catalyst;Solvent;Temperature;
Steps:
1.1
step one,Weigh 18.8g (0.2mol) of phenolFormic acid 11.04g (0.24mol),p-Toluenesulfonic acid 3.8g (0.02mol) andToluene 200mL,Add to the reaction flask with heating jacket and condensation refluxerUnder magnetic stirring,The reaction solution in the reaction flask was heated to 105° C. for 4 hours by heating jacket, and the esterification reaction was performed.Stop heating after esterificationWhen the temperature of the reaction solution drops to 40°C,Then, the reaction solution was distilled, and a fraction at 171°C to 173°C was collected to obtain 24.0 g of colorless phenyl formate with a yield of 98.4% and a purity of 99.2% (GC purity).
References:
Northwest Chemical Institute;Liu Weitao;Zhang Lilong;Wang Xianpei;Zhang Huihui;Li Xiaoan;Yan Jun CN107935834, 2018, A Location in patent:Paragraph 0026; 0032; 0038; 0044
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5312-73-2
31 suppliers
$45.00/100mg
![Phenol](/CAS/20180808/GIF/108-95-2.gif)
108-95-2
725 suppliers
$14.00/25g
![PHENYL FORMATE](/CAS/GIF/1864-94-4.gif)
1864-94-4
89 suppliers
$6.00/1g
![2-phenoxy-1-phenyl-propane-1,3-diol](/CAS/20200401/GIF/70110-65-5.gif)
70110-65-5
7 suppliers
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100-52-7
942 suppliers
$17.30/2g
![PHENYL FORMATE](/CAS/GIF/1864-94-4.gif)
1864-94-4
89 suppliers
$6.00/1g
![Benzoic acid](/CAS/GIF/65-85-0.gif)
65-85-0
1332 suppliers
$10.00/25 g