![](/CAS/GIF/61477-40-5.gif)
(R)-3-amino-1-butanol synthesis
- Product Name:(R)-3-amino-1-butanol
- CAS Number:61477-40-5
- Molecular formula:C4H11NO
- Molecular Weight:89.14
![61477-40-5.png 61477-40-5.png](/NewsImg/2022-09-22/6379943554995799856607856.jpg)
![N-Cbz-(R)-3-amino-1-butanol](/CAS/20180702/GIF/866395-21-3.gif)
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![(R)-3-amino-1-butanol](/CAS/GIF/61477-40-5.gif)
61477-40-5
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Yield:61477-40-5 96%
Reaction Conditions:
with palladium 10% on activated carbon;hydrogen in ethanol at 50 - 60; under 3000.3 - 4500.45 Torr;
Steps:
4 Example 4: Synthesis of (R) -3-aminobutanol
Put 50g (R) -3-benzyloxyamidobutanol in a clean four-necked bottle, add 200ML ethanol, 2.5g10wt% Pd / C, heat up to 50 60 , hydrogen pressure 0.4 0.6MPa, react until the raw materials disappear . After filtration, the filtrate was concentrated under reduced pressure to obtain an oily substance (R) -3-aminobutanol. Yield: 96.0%, purity 99.7%, ee: 99.9%.
References:
CN110683960,2020,A Location in patent:Paragraph 0051; 0052
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3775-73-3
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61477-40-5
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139243-54-2
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![(R)-3-amino-1-butanol](/CAS/GIF/61477-40-5.gif)
61477-40-5
437 suppliers
$15.00/1g